Tag: Solvent

Deuterium oxide NMR- data Chemical shift [ppm] Coupling constants [Hz] 1H 4.72 2J(H,D) 1.0 17O 0.0(Standard )   Physical data Molecular weight [g/mol] 20.03 Density (d420) 1.11 Melting point [°C] 3.8 Boiling point [°C] 101.4 Inflammation temperature [°C] – Refraction index (nD20) 1.328 Dynamic viscosity (20°C) [mPa s] 1.24 Magnetic suszeptibility (20°C) -0.719 x 10^(-6) …

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NMR- data Chemical shift [ppm] (Multiplicity) Coupling constants [Hz] 1H 5.31 (3) 1J(C,D) 27.2 13C 53.7 (5) 2J(H,D) 1.1  H2O/HOD- Shift  1.52   Physical data Formula CD2Cl2 Molecular weight [g/mol] 86.95 Density (d420) 1.36 Melting point [°C] -97 Boiling point [°C] 39 Inflammation temperature [°C] – Refraction index (nD20) 1.4230 Dynamic viscosity (20°C) [mPa s] …

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Dimethylformamide -d7 NMR- data Chemical shift [ppm] (Multiplicity) Coupling constants [Hz] 1H 2.74 (5) 1J(C,D) 20.8 (CD3) 2.91 (5) 29.1 (CDO) 8.02 2J(H,D) 1.9 13C 29.76 (7) 34.89 (7) 163.15 (3) 15N -275.2(NaNO3 = 0) 17O 320(H2O = 0) H2O/HOD SHift 3.45   Physical data Formula C3D7NO Molecular weight [g/mol] 80.14 Density (d420) 1.047 Melting …

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NMR- data Chemical shift [ppm] (Multiplicity) Coupling constants [Hz] 1H 2.5 (5) 1J(C,D) 21.0 (CD3) 13C 39.5 (7) 2J(H,D) 1.9 17O 17(H2O = 0) H2O/HOD Shift 3.3   Physical data Formula C2D6SO Molecular weight [g/mol] 84.17 Density (d420) 1.19 Melting point [°C] 20.2 Boiling point [°C] 190 Inflammation temperature [°C] 95 Refraction index (nD20) 1.4771 …

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NMR- data Chemical shift [ppm] (multiplicity) Coupling constants [Hz] 1H 3.53 (m) 2J(H,D) 21.9 13C 66.66 (5) 17O -3(H2O = 0) H2O/HOD Shift 2.4   Physical data Formula C4D8O2 Molecular weight [g/mol] 96.16 Density (d420) 1.13 Melting point [°C] 11 Boiling point [°C] 100 Inflammation temperature [°C] 12 Refraction index (nD20) 1.4196 Dynamic viscosity (20°C) …

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