Tag: Solvent

NMR- data Chemical shift [ppm] (Multiplicity) Coupling constants [Hz] 1H  11.65 2.04 (5) J(H,D)   2.2 13C  178.99 20 (7) J(C,D) 20  H2O/HDO Shift 11.5 Physical data Formula  C2D4O2 Molecular weight [g/mol]  64.08 Density (d420)  1.119 Melting point [°C]  15.9 Boiling point [°C]  115.5 Inflammation temperature [°C] Refraction index (nD20)  1.368 Dynamic viscosity (20°C) [mPa …

Continue reading

NMR- data Chemical shift [ppm] (multiplicity) Coupling constants [Hz] 1H 2.05 (5) 1J(C,D) 19.4 0.9 13C 29.92 (7) 206.68 (13) 2J(H,D) 2.2  H2O/HOD Shift 2.84/2.81 17O 570   Physical data Formula C3D6O Molecular weight [g/mol] 64.12 Density (d420) 0.87 Melting point [°C] -94.5 Boiling point [°C] 55 Inflammation temperature [°C] -18 Refraction Index (nD20) 1.3565 …

Continue reading

Acetonitrile -d3 NMR- data Chemical shift [ppm] (Multiplicity) Coupling constants [Hz] 1H 1.94 (5) 1J(C,D) 20.7 13C 1.39 (7) 118.69 2J(H,D) 2.5 H2O/HOD Shift 2.12 15N -137.6(CH3NO2 = 0)   Physical data Formula C2D3N Molecular weight [g/mol] 44.05 Density (d420) 0.839 Melting point [°C] -42 Boiling point [°C] 79 Inflammation temperature [°C] 5 Refraction index …

Continue reading

Benzene -d6 NMR- data Chemical shift [ppm] (Mulitiplicity) Coupling constants [Hz] 1H 7.16 1J(C,D) 24.0 13C 128.39 (3) H2O/HOD Shift 0.4 Physical data Formula C6D6 Molecular weight [g/mol] 84.15 Density (d420) 0.948 Melting point [°C] 6.7 Boiling point [°C] 79 Inflammation temperature [°C] -11 Refraction index (nD20) 1.4991 Dynamic viscosity (20°C) [mPa s] 0.69 Magnetic …

Continue reading

NMR- data Chemical shift [ppm] (Multiplicity) Coupling constants [Hz] 1H 7.26 1J(C,D) 32.0 13C 77.23 (3) H2O/HOD Shift 1.55   Physical data Formula CDCl3 Molecular weight [g/mol] 120.38 Density (d420) 1.50 Melting point [°C] -64.1 Boiling point [°C] 60 Inflammation temperature [°C] – Refraction index (nD20) 1.4450 Dynamic viscosity (20°C) [mPa s] 0.57 Magnetic suszeptibility …

Continue reading