{"id":75,"date":"2013-11-06T23:42:12","date_gmt":"2013-11-06T21:42:12","guid":{"rendered":"https:\/\/wissen.science-and-fun.de\/chemistry\/?p=75"},"modified":"2019-01-20T10:14:33","modified_gmt":"2019-01-20T08:14:33","slug":"dichloromethane-d2","status":"publish","type":"post","link":"https:\/\/wissen.science-and-fun.de\/chemistry\/2013\/11\/06\/dichloromethane-d2\/","title":{"rendered":"Dichloromethane-d2"},"content":{"rendered":"\n\n\n\n\n\n\n
\n

NMR- data<\/h3>\n<\/td>\n<\/tr>\n

\"[Picture]\"<\/td>\nChemical shift [ppm] (Multiplicity)<\/td>\nCoupling constants [Hz]<\/td>\n<\/td>\n<\/tr>\n
1<\/sup>H<\/td>\n5.31 (3)<\/td>\n1<\/sup>J(C,D)<\/td>\n27.2<\/td>\n<\/tr>\n
13<\/sup>C<\/td>\n53.7 (5)<\/td>\n2<\/sup>J(H,D)<\/td>\n1.1<\/td>\n<\/tr>\n
 H2<\/sub>O\/HOD- Shift<\/td>\n 1.52<\/td>\n<\/td>\n<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n

 
\n<\/p>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
\n

Physical data<\/h3>\n<\/td>\n<\/tr>\n

Formula<\/td>\nCD2<\/sub>Cl2<\/sub><\/td>\n<\/tr>\n
Molecular weight [g\/mol]<\/td>\n86.95<\/td>\n<\/tr>\n
Density (d4<\/sub>20<\/sup>)<\/td>\n1.36<\/td>\n<\/tr>\n
Melting point [\u00b0C]<\/td>\n-97<\/td>\n<\/tr>\n
Boiling point [\u00b0C]<\/td>\n39<\/td>\n<\/tr>\n
Inflammation temperature [\u00b0C]<\/td>\n–<\/td>\n<\/tr>\n
Refraction index (nD<\/sub>20<\/sup>)<\/td>\n1.4230<\/td>\n<\/tr>\n
Dynamic viscosity (20\u00b0C) [mPa s]<\/td>\n0.43<\/td>\n<\/tr>\n
Magnetic suszeptibility (20\u00b0C)<\/td>\n-0.733 x 10^(-6)<\/td>\n<\/tr>\n
Dielectrical constant<\/td>\n8.93<\/td>\n<\/tr>\n
Dipole momentum [D]<\/td>\n1.5<\/td>\n<\/tr>\n
Polarity [kJ\/mol]<\/td>\n172.0<\/td>\n<\/tr>\n
Donor strength [kJ\/mol]<\/td>\n10.0<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n\n\n

Common impurities<\/h3>\n\n\n\n\n\n\n\t\n\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t
compound<\/th>proton<\/th>multiplicity<\/th>1H-shift [ppm]<\/th>carbon<\/th>13C-shift [ppm]<\/th>\n<\/tr>\n<\/thead>\n
water<\/td>OH<\/td>s<\/td>1.52<\/td>x<\/td>x<\/td>\n<\/tr>\n
acetic acid<\/td>CH 3<\/td>s<\/td>2.06<\/td>CH 3<\/td>20.91<\/td>\n<\/tr>\n
<\/td><\/td><\/td>CO<\/td>175.85<\/td>\n<\/tr>\n
acetone<\/td>CH 3<\/td>s<\/td>2.12<\/td>CH 3<\/td>31<\/td>\n<\/tr>\n
<\/td><\/td><\/td>CO<\/td>206.78<\/td>\n<\/tr>\n
acetonitrile<\/td>CH 3<\/td>s<\/td>1.97<\/td>CH 3<\/td>2.03<\/td>\n<\/tr>\n
<\/td><\/td><\/td>CN<\/td>116.92<\/td>\n<\/tr>\n
benzene<\/td>CH<\/td>s<\/td>7.35<\/td>CH<\/td>128.68<\/td>\n<\/tr>\n
t-butyl-alcohol<\/td>CH 3<\/td>s<\/td>1.24<\/td>CH 3<\/td>31.46<\/td>\n<\/tr>\n
OH<\/td>s<\/td><\/td>C -CH 3<\/td>69.11<\/td>\n<\/tr>\n
carbon dioxide<\/td><\/td><\/td><\/td>CO 2<\/td>125.26<\/td>\n<\/tr>\n
carbon disulfide<\/td><\/td><\/td><\/td>CS 2<\/td>192.95<\/td>\n<\/tr>\n
carbon tetrachloride<\/td><\/td><\/td><\/td>CCl 4<\/td>96.52<\/td>\n<\/tr>\n
chloroform<\/td>CH<\/td>s<\/td>7.32<\/td>CH<\/td>77.99<\/td>\n<\/tr>\n
18-crown-6<\/td>CH 2<\/td>s<\/td>3.59<\/td>CH 2<\/td>70.47<\/td>\n<\/tr>\n
cyclohexane<\/td>CH 2<\/td>s<\/td>1.44<\/td>CH 2<\/td>27.38<\/td>\n<\/tr>\n
1,2-dichloroethane<\/td>CH 2<\/td>s<\/td>3.76<\/td>CH 2<\/td>44.35<\/td>\n<\/tr>\n
dichloromethane<\/td>CH 2<\/td>s<\/td>5.33<\/td>CH 2<\/td>54.24<\/td>\n<\/tr>\n
diethylether<\/td>CH 3<\/td>t<\/td>1.15<\/td>CH 3<\/td>15.44<\/td>\n<\/tr>\n
CH 2<\/td>q<\/td>3.43<\/td>CH 2<\/td>66.11<\/td>\n<\/tr>\n
1,4-dioxane<\/td>CH 2<\/td>s<\/td>3.65<\/td>CH 2<\/td>67.47<\/td>\n<\/tr>\n
diglyme<\/td>CH 2<\/td>m<\/td>3.57<\/td>CH 2<\/td>72.25<\/td>\n<\/tr>\n
CH 2<\/td>m<\/td>3.5<\/td>CH 2<\/td>70.7<\/td>\n<\/tr>\n
OCH 3<\/td>s<\/td>3.28<\/td>OCH 3<\/td>58.95<\/td>\n<\/tr>\n
DME<\/td>CH 3<\/td>s<\/td>3.34<\/td>CH 3<\/td>59.02<\/td>\n<\/tr>\n
CH 2<\/td>s<\/td>3.49<\/td>CH 2<\/td>72.24<\/td>\n<\/tr>\n
dimethylformamide<\/td>CH<\/td>s<\/td>7.91<\/td>CH<\/td>162.57<\/td>\n<\/tr>\n
CH 3<\/td>s<\/td>2.88<\/td>CH 3<\/td>36.56<\/td>\n<\/tr>\n
CH 3<\/td>s<\/td>2.76<\/td>CH 3<\/td>31.39<\/td>\n<\/tr>\n
ethane<\/td>CH 3<\/td>s<\/td>0.85<\/td>CH 3<\/td>6.91<\/td>\n<\/tr>\n
ethylene<\/td>CH 2<\/td>s<\/td>5.4<\/td>CH 2<\/td>123.2<\/td>\n<\/tr>\n
ethanol<\/td>CH 3<\/td>t<\/td>1.19<\/td>CH 3<\/td>18.69<\/td>\n<\/tr>\n
CH 2<\/td>q<\/td>3.66<\/td>CH 2<\/td>58.57<\/td>\n<\/tr>\n
OH<\/td>s<\/td>1.33<\/td>x<\/td>x<\/td>\n<\/tr>\n
ethylene glycol<\/td>CH 2<\/td>s<\/td>3.66<\/td>CH 2<\/td>64.08<\/td>\n<\/tr>\n
ethyl acetate<\/td>CH3CO<\/td>s<\/td>2<\/td>CH3CO<\/td>21.15<\/td>\n<\/tr>\n
<\/td><\/td><\/td>CO<\/td>171.24<\/td>\n<\/tr>\n
C H2 CH3<\/td>q<\/td>4.08<\/td>C H2 CH3<\/td>60.63<\/td>\n<\/tr>\n
CH 2 C H 3<\/td>t<\/td>1.23<\/td>CH 2 C H 3<\/td>14.37<\/td>\n<\/tr>\n
H grease<\/td>CH 3<\/td>m<\/td>0,84-0,90<\/td>x<\/td>x<\/td>\n<\/tr>\n
CH 2<\/td>broad<\/td>1.27<\/td>CH 2<\/td>30.14<\/td>\n<\/tr>\n
hexamethylbenzene<\/td>CH 3<\/td>s<\/td>2.2<\/td>CH 3<\/td>16.71<\/td>\n<\/tr>\n
<\/td><\/td><\/td>C<\/td>132.09<\/td>\n<\/tr>\n
n-hexane<\/td>CH 3<\/td>t<\/td>0.89<\/td>CH 3<\/td>14.28<\/td>\n<\/tr>\n
CH 2<\/td>m<\/td>1.27<\/td>CH 2 (2,5)<\/td>23.07<\/td>\n<\/tr>\n
<\/td><\/td><\/td>CH 2 (3,4)<\/td>32.01<\/td>\n<\/tr>\n
HMDSO<\/td>CH 3<\/td>s<\/td>0.07<\/td>CH 3<\/td>1.96<\/td>\n<\/tr>\n
HMPA<\/td>CH 3<\/td>d<\/td>2.6<\/td>CH 3<\/td>36.99<\/td>\n<\/tr>\n
hydrogen<\/td>H 2<\/td>s<\/td>4.59<\/td>x<\/td>x<\/td>\n<\/tr>\n
imidazole<\/td>CH(2)<\/td>s<\/td>7.63<\/td>CH(2)<\/td>135.76<\/td>\n<\/tr>\n
CH(4,5)<\/td>s<\/td>7.07<\/td>CH(4,5)<\/td>122.16<\/td>\n<\/tr>\n
methane<\/td>CH 4<\/td>s<\/td>0.21<\/td>CH 4<\/td>-4.33<\/td>\n<\/tr>\n
methanol<\/td>CH 3<\/td>s<\/td>3.42<\/td>CH 3<\/td>50.45<\/td>\n<\/tr>\n
OH<\/td>s<\/td>1.09<\/td>x<\/td>x<\/td>\n<\/tr>\n
nitromethane<\/td>CH 3<\/td>s<\/td>4.31<\/td>CH 3<\/td>63.03<\/td>\n<\/tr>\n
n-pentane<\/td>CH 3<\/td>t<\/td>0.89<\/td>CH 3<\/td>14.24<\/td>\n<\/tr>\n
CH 2<\/td>m<\/td>1.3<\/td>CH 2 (2,4)<\/td>22.77<\/td>\n<\/tr>\n
<\/td><\/td><\/td>CH 2 (3)<\/td>34.57<\/td>\n<\/tr>\n
propane<\/td>CH 3<\/td>t<\/td>0.9<\/td>CH 3<\/td>16.63<\/td>\n<\/tr>\n
CH 2<\/td>septett<\/td>1.32<\/td>CH 2<\/td>16.63<\/td>\n<\/tr>\n
2-propanol<\/td>CH 3<\/td>d<\/td>1.17<\/td>CH 3<\/td>25.43<\/td>\n<\/tr>\n
CH<\/td>septett<\/td>3.97<\/td>CH<\/td>64.67<\/td>\n<\/tr>\n
propylene<\/td>CH3<\/td>d<\/td>1.71<\/td>CH3<\/td>19.47<\/td>\n<\/tr>\n
CH 2 (1)<\/td>m<\/td>4.93<\/td>CH 2<\/td>115.7<\/td>\n<\/tr>\n
CH 2 (2)<\/td>m<\/td>5.03<\/td>x<\/td>x<\/td>\n<\/tr>\n
CH<\/td>m<\/td>5.84<\/td>CH<\/td>134.21<\/td>\n<\/tr>\n
pyridine<\/td>CH(2,6)<\/td>m<\/td>8.59<\/td>CH(2,6)<\/td>150.27<\/td>\n<\/tr>\n
CH(3,5)<\/td>m<\/td>7.28<\/td>CH(3,5)<\/td>124.06<\/td>\n<\/tr>\n
CH(4)<\/td>m<\/td>7.68<\/td>CH(4)<\/td>136.16<\/td>\n<\/tr>\n
pyrrole<\/td>NH<\/td>broad<\/td>8.69<\/td>x<\/td>x<\/td>\n<\/tr>\n
CH (2,5)<\/td>m<\/td>6.79<\/td>CH (2,5)<\/td>117.93<\/td>\n<\/tr>\n
CH (3,4)<\/td>m<\/td>6.19<\/td>CH (3,4)<\/td>108.02<\/td>\n<\/tr>\n
pyrrolidine<\/td>CH 2 (2,5)<\/td>m<\/td>2.82<\/td>CH 2 (2,5)<\/td>47.02<\/td>\n<\/tr>\n
CH 2 (3,4)<\/td>m<\/td>1.67<\/td>CH 2 (3,4)<\/td>25.83<\/td>\n<\/tr>\n
silicon grease<\/td>CH 3<\/td>s<\/td>0.09<\/td>CH 3<\/td>1.22<\/td>\n<\/tr>\n
tetrahydrofuran<\/td>CH 2 (2,5)<\/td>m<\/td>3.69<\/td>CH 2 (2,5)<\/td>68.16<\/td>\n<\/tr>\n
CH 2 (3,4)<\/td>m<\/td>1.82<\/td>CH 2 (3,4)<\/td>25.98<\/td>\n<\/tr>\n
Toluene<\/td>CH 3<\/td>s<\/td>2.31<\/td>CH 3<\/td>21.53<\/td>\n<\/tr>\n
<\/td><\/td><\/td>C(1)<\/td>138.36<\/td>\n<\/tr>\n
CH (2,4,6)<\/td>m<\/td>7.15<\/td>CH (2,6)<\/td>129.35<\/td>\n<\/tr>\n
CH (3,5)<\/td>m<\/td>7.24<\/td>CH (3,5)<\/td>128.54<\/td>\n<\/tr>\n
<\/td><\/td><\/td>CH (4)<\/td>125.62<\/td>\n<\/tr>\n
triethylamine<\/td>CH 3<\/td>t<\/td>0.99<\/td>CH 3<\/td>12.12<\/td>\n<\/tr>\n
CH 2<\/td>q<\/td>2.48<\/td>CH 2<\/td>46.75<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\nThe table was taken from German. The comma is therefore the decimal point.
\nFor example, 4.3 stands for the English 4.3.
\n
\nSource:
\nNMR Chemical Shifts of Trace Impurities: Common Laboratory Solvents, Organics, and Gases in Deuterated Solvents Relevant to the Organometallic Chemist\t
\nGregory R. Fulmer, Alexander J. M. Miller, Nathaniel H. Sherden, Hugo E. Gottlieb, Abraham Nudelman, Brian M. Stoltz, John E. Bercaw and Karen I. Goldberg\t
\nOrganometallics, 2010, 29 (9), pp 2176\u20132179\t
\nDOI: 10.1021\/om100106e\t<\/span>\n\n","protected":false},"excerpt":{"rendered":"

NMR- data Chemical shift [ppm] (Multiplicity) Coupling constants [Hz] 1H 5.31 (3) 1J(C,D) 27.2 13C 53.7 (5) 2J(H,D) 1.1  H2O\/HOD- Shift  1.52   Physical data Formula CD2Cl2 Molecular weight [g\/mol] 86.95 Density (d420) 1.36 Melting point [\u00b0C] -97 Boiling point [\u00b0C] 39 Inflammation temperature [\u00b0C] – Refraction index (nD20) 1.4230 Dynamic viscosity (20\u00b0C) [mPa s] … <\/p>\n

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