{"id":51,"date":"2013-11-06T22:25:17","date_gmt":"2013-11-06T20:25:17","guid":{"rendered":"https:\/\/wissen.science-and-fun.de\/chemistry\/?p=51"},"modified":"2019-01-19T21:58:42","modified_gmt":"2019-01-19T19:58:42","slug":"tetrahydrofurane-d8","status":"publish","type":"post","link":"https:\/\/wissen.science-and-fun.de\/chemistry\/2013\/11\/06\/tetrahydrofurane-d8\/","title":{"rendered":"Tetrahydrofurane-d8"},"content":{"rendered":"\n\n\n\n\n\n\n\n\n\n
\n

NMR- data<\/h3>\n<\/td>\n<\/tr>\n

\"[Picture]\"<\/td>\nChemical shift [ppm]<\/td>\nCoupling constants [Hz]<\/td>\n<\/td>\n<\/tr>\n
1<\/sup>H<\/td>\n1.72<\/td>\n1<\/sup>J(C,D)<\/td>\n22.0 (C-1)<\/td>\n<\/tr>\n
3.57<\/td>\n20.5 (C-2)<\/td>\n<\/tr>\n
13<\/sup>C<\/td>\n25.2<\/td>\n<\/tr>\n
67.2<\/td>\n<\/tr>\n
17<\/sup>O<\/td>\n16(H2<\/sub>O = 0)<\/span><\/td>\n<\/tr>\n
H2<\/sub>O\/HOD<\/td>\n2.42<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n

 
\n<\/p>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
\n

Physical data<\/h3>\n<\/td>\n<\/tr>\n

Formula<\/td>\nC4<\/sub>D8<\/sub>O<\/td>\n<\/tr>\n
Molecular weight [g\/mol]<\/td>\n80.15<\/td>\n<\/tr>\n
Density (d4<\/sub>20<\/sup>)<\/td>\n0.99<\/td>\n<\/tr>\n
Melting point [\u00b0C]<\/td>\n-108.5<\/td>\n<\/tr>\n
Boiling point [\u00b0C]<\/td>\n64<\/td>\n<\/tr>\n
Inflammation temperature [\u00b0C]<\/td>\n-17.5<\/td>\n<\/tr>\n
Refraction index (nD<\/sub>20<\/sup>)<\/td>\n1.4043<\/td>\n<\/tr>\n
Dynamic viscosity (20\u00b0C) [mPa s]<\/td>\n0.47<\/td>\n<\/tr>\n
Magnetic suszeptibility (20\u00b0C)<\/td>\n-0.6 x 10-6<\/sup><\/td>\n<\/tr>\n
Dielectrical constant<\/td>\n7.6<\/td>\n<\/tr>\n
Dipole momentum [D]<\/td>\n1.7<\/td>\n<\/tr>\n
Polarity [kJ\/mol]<\/td>\n156.5<\/td>\n<\/tr>\n
Donor strength [kJ\/mol]<\/td>\n90.4<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n\n\n

Common impurities<\/h3>\n\n\n\n\n\n\n\t\n\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t
compound<\/th>proton<\/th>multiplicity<\/th>1H-shift [ppm]<\/th>carbon<\/th>13C-shift [ppm]<\/th>\n<\/tr>\n<\/thead>\n
water<\/td>OH<\/td>s<\/td>2.46<\/td><\/td><\/td>\n<\/tr>\n
acetic acid<\/td>CH3<\/sub><\/td>s<\/td>1.89<\/td>CH3<\/td>20.13<\/td>\n<\/tr>\n
<\/td><\/td><\/td>CO<\/td>171.69<\/td>\n<\/tr>\n
acetone<\/td>CH3<\/td>s<\/td>2.05<\/td>CH 3<\/td>30.17<\/td>\n<\/tr>\n
<\/td><\/td><\/td>CO<\/td>204.19<\/td>\n<\/tr>\n
acetonitrile<\/td>CH3<\/td>s<\/td>1.95<\/td>CH 3<\/td>0.45<\/td>\n<\/tr>\n
<\/td><\/td><\/td>CN<\/td>116.79<\/td>\n<\/tr>\n
benzene<\/td>CH<\/td>s<\/td>7.31<\/td>CH<\/td>128.84<\/td>\n<\/tr>\n
t-butyl-alcohol<\/td>CH3<\/td>s<\/td>1.15<\/td>CH 3<\/td>30.57<\/td>\n<\/tr>\n
OH<\/td>s<\/td>3.16<\/td>C -CH 3<\/td>67.5<\/td>\n<\/tr>\n
carbon dioxide<\/td><\/td><\/td><\/td>CO 2<\/td>125.69<\/td>\n<\/tr>\n
carbon disulfide<\/td><\/td><\/td><\/td>CS 2<\/td>193.37<\/td>\n<\/tr>\n
carbon tetrachloride<\/td><\/td><\/td><\/td>CCl 4<\/td>96.89<\/td>\n<\/tr>\n
chloroform<\/td>CH<\/td>s<\/td>7.89<\/td>CH<\/td>79.24<\/td>\n<\/tr>\n
18-crown-6<\/td>CH2<\/td>s<\/td>3.57<\/td>CH 2<\/td>71.34<\/td>\n<\/tr>\n
cyclohexane<\/td>CH2<\/td>s<\/td>1.44<\/td>CH 2<\/td>27.58<\/td>\n<\/tr>\n
1,2-dichloroethane<\/td>CH 2<\/td>s<\/td>3.77<\/td>CH 2<\/td>44.64<\/td>\n<\/tr>\n
dichloromethane<\/td>CH 2<\/td>s<\/td>5.51<\/td>CH 2<\/td>54.67<\/td>\n<\/tr>\n
diethylether<\/td>CH 3<\/td>t<\/td>1.12<\/td>CH 3<\/td>15.49<\/td>\n<\/tr>\n
CH 2<\/td>q<\/td>3.38<\/td>CH 2<\/td>66.14<\/td>\n<\/tr>\n
1,4-dioxane<\/td>CH 2<\/td>s<\/td>3.56<\/td>CH 2<\/td>67.65<\/td>\n<\/tr>\n
diglyme<\/td>CH 2<\/td>m<\/td>3.43<\/td>CH 2<\/td>71.17<\/td>\n<\/tr>\n
CH 2<\/td>m<\/td>3.53<\/td>CH 2<\/td>72.72<\/td>\n<\/tr>\n
OCH 3<\/td>s<\/td>3.28<\/td>OCH 3<\/td>58.72<\/td>\n<\/tr>\n
DME<\/td>CH 3<\/td>s<\/td>3.28<\/td>CH 3<\/td>58.72<\/td>\n<\/tr>\n
CH 2<\/td>s<\/td>3.43<\/td>CH 2<\/td>72.58<\/td>\n<\/tr>\n
dimethylformamide<\/td>CH<\/td>s<\/td>7.91<\/td>CH<\/td>161.96<\/td>\n<\/tr>\n
CH 3<\/td>s<\/td>2.88<\/td>CH 3<\/td>35.65<\/td>\n<\/tr>\n
CH 3<\/td>s<\/td>2.76<\/td>CH 3<\/td>30.7<\/td>\n<\/tr>\n
ethane<\/td>CH 3<\/td>s<\/td>0.85<\/td>CH 3<\/td>6.79<\/td>\n<\/tr>\n
ethylene<\/td>CH 2<\/td>s<\/td>5.36<\/td>CH 2<\/td>123.09<\/td>\n<\/tr>\n
ethanol<\/td>CH 3<\/td>t<\/td>1.1<\/td>CH 3<\/td>18.9<\/td>\n<\/tr>\n
CH 2<\/td>q<\/td>3.51<\/td>CH 2<\/td>57.6<\/td>\n<\/tr>\n
OH<\/td>s<\/td>3.3<\/td>x<\/td>x<\/td>\n<\/tr>\n
ethylene glycol<\/td>CH 2<\/td>s<\/td>3.48<\/td>CH 2<\/td>64.35<\/td>\n<\/tr>\n
ethyl acetate<\/td>CH3CO<\/td>s<\/td>1.94<\/td>CH3CO<\/td>20.45<\/td>\n<\/tr>\n
<\/td><\/td><\/td>CO<\/td>170.32<\/td>\n<\/tr>\n
C H2 CH3<\/td>q<\/td>4.04<\/td>C H2 CH3<\/td>60.3<\/td>\n<\/tr>\n
CH 2 C H 3<\/td>t<\/td>1.19<\/td>CH 2 C H 3<\/td>14.37<\/td>\n<\/tr>\n
H grease<\/td>CH 3<\/td>m<\/td>0,85-0,91<\/td>x<\/td>x<\/td>\n<\/tr>\n
CH 2<\/td>broad<\/td>1.29<\/td>CH 2<\/td>30.45<\/td>\n<\/tr>\n
hexamethylbenzene<\/td>CH 3<\/td>s<\/td>2.18<\/td>CH 3<\/td>16.71<\/td>\n<\/tr>\n
<\/td><\/td><\/td>C<\/td>131.88<\/td>\n<\/tr>\n
n-hexane<\/td>CH 3<\/td>t<\/td>0.89<\/td>CH 3<\/td>14.22<\/td>\n<\/tr>\n
CH 2<\/td>m<\/td>1.29<\/td>CH 2 (2,5)<\/td>23.33<\/td>\n<\/tr>\n
<\/td><\/td><\/td>CH 2 (3,4)<\/td>32.34<\/td>\n<\/tr>\n
HMDSO<\/td>CH 3<\/td>s<\/td>0.07<\/td>CH 3<\/td>1.83<\/td>\n<\/tr>\n
HMPA<\/td>CH 3<\/td>d<\/td>2.58<\/td>CH 3<\/td>36.89<\/td>\n<\/tr>\n
hydrogen<\/td>H 2<\/td>s<\/td>4.55<\/td>x<\/td>x<\/td>\n<\/tr>\n
imidazole<\/td>CH(2)<\/td>s<\/td>7.48<\/td>CH(2)<\/td>135.72<\/td>\n<\/tr>\n
CH(4,5)<\/td>s<\/td>6.94<\/td>CH(4,5)<\/td>122.2<\/td>\n<\/tr>\n
methane<\/td>CH 4<\/td>s<\/td>0.19<\/td>CH 4<\/td>-4.9<\/td>\n<\/tr>\n
methanol<\/td>CH 3<\/td>s<\/td>3.27<\/td>CH 3<\/td>49.64<\/td>\n<\/tr>\n
OH<\/td>s<\/td>3.02<\/td>x<\/td>x<\/td>\n<\/tr>\n
nitromethane<\/td>CH 3<\/td>s<\/td>4.31<\/td>CH 3<\/td>62.49<\/td>\n<\/tr>\n
n-pentane<\/td>CH 3<\/td>t<\/td>0.89<\/td>CH 3<\/td>14.18<\/td>\n<\/tr>\n
CH 2<\/td>m<\/td>1.31<\/td>CH 2 (2,4)<\/td>23<\/td>\n<\/tr>\n
<\/td><\/td><\/td>CH 2 (3)<\/td>34.87<\/td>\n<\/tr>\n
propane<\/td>CH 3<\/td>t<\/td>0.9<\/td>CH 3<\/td>16.6<\/td>\n<\/tr>\n
CH 2<\/td>septett<\/td>1.33<\/td>CH 2<\/td>16.82<\/td>\n<\/tr>\n
2-propanol<\/td>CH 3<\/td>d<\/td>1.08<\/td>CH 3<\/td>25.7<\/td>\n<\/tr>\n
CH<\/td>septett<\/td>3.82<\/td>CH<\/td>66.14<\/td>\n<\/tr>\n
propylene<\/td>CH3<\/td>d<\/td>1.69<\/td>CH3<\/td>19.27<\/td>\n<\/tr>\n
CH 2 (1)<\/td>m<\/td>4.89<\/td>CH 2<\/td>115.74<\/td>\n<\/tr>\n
CH 2 (2)<\/td>m<\/td>4.99<\/td>x<\/td>x<\/td>\n<\/tr>\n
CH<\/td>m<\/td>5.79<\/td>CH<\/td>134.02<\/td>\n<\/tr>\n
pyridine<\/td>CH(2,6)<\/td>m<\/td>8.54<\/td>CH(2,6)<\/td>150.57<\/td>\n<\/tr>\n
CH(3,5)<\/td>m<\/td>7.25<\/td>CH(3,5)<\/td>124.08<\/td>\n<\/tr>\n
CH(4)<\/td>m<\/td>7.65<\/td>CH(4)<\/td>135.99<\/td>\n<\/tr>\n
pyrrole<\/td>NH<\/td>broad<\/td>9.96<\/td>x<\/td>x<\/td>\n<\/tr>\n
CH (2,5)<\/td>m<\/td>6.66<\/td>CH (2,5)<\/td>118.03<\/td>\n<\/tr>\n
CH (3,4)<\/td>m<\/td>6.02<\/td>CH (3,4)<\/td>107.74<\/td>\n<\/tr>\n
pyrrolidine<\/td>CH 2 (2,5)<\/td>m<\/td>2.75<\/td>CH 2 (2,5)<\/td>45.82<\/td>\n<\/tr>\n
CH 2 (3,4)<\/td>m<\/td>1.59<\/td>CH 2 (3,4)<\/td>26.17<\/td>\n<\/tr>\n
silicon grease<\/td>CH 3<\/td>s<\/td>0.11<\/td>CH 3<\/td>1.2<\/td>\n<\/tr>\n
tetrahydrofuran<\/td>CH 2 (2,5)<\/td>m<\/td>3.62<\/td>CH 2 (2,5)<\/td>68.03<\/td>\n<\/tr>\n
CH 2 (3,4)<\/td>m<\/td>1.79<\/td>CH 2 (3,4)<\/td>26.19<\/td>\n<\/tr>\n
Toluene<\/td>CH 3<\/td>s<\/td>2.31<\/td>CH 3<\/td>21.29<\/td>\n<\/tr>\n
<\/td><\/td><\/td>C(1)<\/td>138.24<\/td>\n<\/tr>\n
CH (2,4,6)<\/td>m<\/td>7.1<\/td>CH (2,6)<\/td>129.47<\/td>\n<\/tr>\n
CH (3,5)<\/td>m<\/td>7.19<\/td>CH (3,5)<\/td>128.71<\/td>\n<\/tr>\n
<\/td><\/td><\/td>CH (4)<\/td>125.84<\/td>\n<\/tr>\n
triethylamine<\/td>CH 3<\/td>t<\/td>0.97<\/td>CH 3<\/td>12.51<\/td>\n<\/tr>\n
CH 2<\/td>q<\/td>2.46<\/td>CH 2<\/td>47.18<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\nThe table was taken from German. The comma is therefore the decimal point.
\nFor example, 4.3 stands for the English 4.3.
\n
\nSource:
\nNMR Chemical Shifts of Trace Impurities: Common Laboratory Solvents, Organics, and Gases in Deuterated Solvents Relevant to the Organometallic Chemist\t\t\t\t\t\t\t\t\t\t\t\t
\nGregory R. Fulmer,\u00a0Alexander J. M. Miller,\u00a0Nathaniel H. Sherden,\u00a0Hugo E. Gottlieb,\u00a0Abraham Nudelman,\u00a0Brian M. Stoltz,\u00a0John E. Bercaw\u00a0and\u00a0Karen I. Goldberg\t\t\t\t\t\t\t\t\t\t\t\t\t
\nOrganometallics,\u00a02010,\u00a029\u00a0(9), pp 2176\u20132179\t\t\t\t
\nDOI:\u00a010.1021\/om100106e\t\t\t\t\t\t\t\t\t\t\t\t
\n<\/span>\n\n","protected":false},"excerpt":{"rendered":"

NMR- data Chemical shift [ppm] Coupling constants [Hz] 1H 1.72 1J(C,D) 22.0 (C-1) 3.57 20.5 (C-2) 13C 25.2 67.2 17O 16(H2O = 0) H2O\/HOD 2.42   Physical data Formula C4D8O Molecular weight [g\/mol] 80.15 Density (d420) 0.99 Melting point [\u00b0C] -108.5 Boiling point [\u00b0C] 64 Inflammation temperature [\u00b0C] -17.5 Refraction index (nD20) 1.4043 Dynamic viscosity … <\/p>\n

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