{"id":1554,"date":"2017-04-09T17:27:58","date_gmt":"2017-04-09T15:27:58","guid":{"rendered":"https:\/\/wissen.science-and-fun.de\/chemistry\/?p=1554"},"modified":"2017-04-29T07:50:01","modified_gmt":"2017-04-29T05:50:01","slug":"lysine-lys-k","status":"publish","type":"post","link":"https:\/\/wissen.science-and-fun.de\/chemistry\/2017\/04\/09\/lysine-lys-k\/","title":{"rendered":"Lysine (Lys, K)"},"content":{"rendered":"

NMR- data [1] of lysine:<\/h3>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
\"Lysin\"<\/th>\nAtom<\/th>\nAtomtyp<\/th>\nChemical shift [ppm]1<\/sup><\/th>\nRandom Coil
\nchem. shift3<\/sup><\/th>\n		Random Coil
\nchem. shift4<\/sup><\/th>\n<\/tr>\n
average<\/strong><\/td>\n\u03c35<\/sup><\/strong><\/td>\nentries2<\/sup><\/strong><\/td>\n<\/tr>\n
H<\/td>\nH<\/td>\n\u00a08.178<\/td>\n\u00a00.664<\/td>\n\u00a058906<\/td>\n\u00a08.29<\/td>\n\u00a08.18<\/td>\n<\/tr>\n
H\u03b1<\/td>\nH<\/td>\n\u00a04.264<\/td>\n\u00a00.466<\/td>\n\u00a045467<\/td>\n\u00a04.32<\/td>\n\u00a04.60<\/td>\n<\/tr>\n
H\u03b22<\/td>\nH<\/td>\n\u00a01.774<\/td>\n\u00a00.319<\/td>\n\u00a041062<\/td>\n\u00a01.84<\/td>\n\u00a01.80<\/td>\n<\/tr>\n
H\u03b23<\/td>\nH<\/td>\n\u00a01.744<\/td>\n\u00a00.334<\/td>\n\u00a038519<\/td>\n\u00a01.75<\/td>\n\u00a01.74<\/td>\n<\/tr>\n
H\u03b32<\/td>\nH<\/td>\n\u00a01.364<\/td>\n\u00a00.312<\/td>\n\u00a037233<\/td>\n\u00a01.44<\/td>\n\u00a01.45<\/td>\n<\/tr>\n
H\u03b33<\/td>\nH<\/td>\n\u00a01.348<\/td>\n\u00a00.326<\/td>\n\u00a034123<\/td>\n\u00a01.44<\/td>\n\u00a01.45<\/td>\n<\/tr>\n
H\u03b42<\/td>\nH<\/td>\n\u00a01.609<\/td>\n\u00a00.751<\/td>\n\u00a033176<\/td>\n\u00a01.68<\/td>\n\u00a01.69<\/td>\n<\/tr>\n
H\u03b43<\/td>\nH<\/td>\n\u00a01.595<\/td>\n\u00a00.369<\/td>\n\u00a029506<\/td>\n\u00a01.68<\/td>\n\u00a01.69<\/td>\n<\/tr>\n
H\u03b52<\/td>\nH<\/td>\n\u00a02.910<\/td>\n\u00a00.217<\/td>\n\u00a032694<\/td>\n\u00a02.99<\/td>\n\u00a02.97<\/td>\n<\/tr>\n
H\u03b53<\/td>\nH<\/td>\n\u00a02.903<\/td>\n\u00a00.223<\/td>\n\u00a028496<\/td>\n\u00a02.99<\/td>\n\u00a02.97<\/td>\n<\/tr>\n
H\u03b6<\/td>\nH<\/td>\n\u00a07.313<\/td>\n\u00a01.147<\/td>\n\u00a01284<\/td>\n\u00a07.81<\/td>\n\u00a07.81<\/td>\n<\/tr>\n
C<\/td>\nC<\/td>\n\u00a0176.591<\/td>\n\u00a06.358<\/td>\n\u00a036173<\/td>\n\u00a0176.6<\/td>\n\u00a0174.8<\/td>\n<\/tr>\n
C\u03b1<\/td>\nC<\/td>\n\u00a056.935<\/td>\n\u00a02.272<\/td>\n\u00a050111<\/td>\n\u00a056.2<\/td>\n\u00a054.2<\/td>\n<\/tr>\n
C\u03b2<\/td>\nC<\/td>\n\u00a032.810<\/td>\n\u00a02.227<\/td>\n\u00a046864<\/td>\n\u00a033.1<\/td>\n\u00a032.6<\/td>\n<\/tr>\n
C\u03b3<\/td>\nC<\/td>\n\u00a024.918<\/td>\n\u00a01.615<\/td>\n\u00a031094<\/td>\n\u00a024.7<\/td>\n\u00a024.6<\/td>\n<\/tr>\n
C\u03b4<\/td>\nC<\/td>\n\u00a028.969<\/td>\n\u00a01.507<\/td>\n\u00a029403<\/td>\n\u00a029.0<\/td>\n\u00a029.1<\/td>\n<\/tr>\n
C\u03b5<\/td>\nC<\/td>\n\u00a041.896<\/td>\n\u00a01.451<\/td>\n\u00a025495<\/td>\n\u00a041.9<\/td>\n\u00a041.9<\/td>\n<\/tr>\n
N<\/td>\nN<\/td>\n\u00a0121.023<\/td>\n\u00a04.225<\/td>\n\u00a054081<\/td>\n\u00a0120.4<\/td>\n\u00a0121.6<\/td>\n<\/tr>\n
N\u03b6<\/td>\nN<\/td>\n\u00a048.135<\/td>\n\u00a030.664<\/td>\n\u00a0208<\/td>\n\u00a0125.9<\/td>\n\u00a0125.9<\/td>\n<\/tr>\n
proportion of proteines<\/th>\npK2<\/sub> COOH<\/th>\npK1<\/sub>COOH<\/th>\nisoelectrical
\npoint<\/th>\n		pK1<\/sub>NH2<\/sub><\/th>\npK2<\/sub>NH2<\/sub><\/th>\n<\/tr>\n
\u00a07.0%<\/td>\n–<\/td>\n\u00a02.20<\/td>\n\u00a09.59<\/td>\n\u00a08.90<\/td>\n\u00a010.28<\/td>\n<\/tr>\n
CAS- number<\/th>\nmolar mass<\/th>\nformula<\/th>\ndensity<\/th>\nmelting point<\/th>\nsolubility<\/th>\n<\/tr>\n
\n
    \n
  • 56-87-1 (L<\/small>-Enantiomer)<\/li>\n
  • 923-27-3 (D<\/small>-Enantiomer)<\/li>\n
  • 70-54-2 (Racemat)<\/li>\n
  • 657-27-2 (Monohydrochlorid)<\/li>\n<\/ul>\n<\/td>\n
\u00a0146,19\u00a0g\u00b7mol\u22121<\/sup><\/td>\n\u00a0C6<\/sub>H14<\/sub>N2<\/sub>O2<\/sub><\/td>\n<\/td>\n\n<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n
\n

1<\/sup> Depending on the type of atom it was 1<\/sup>H, 13<\/sup>C or 15<\/sup>N chemical shift. 1<\/sup>H und 13<\/sup>C relative to TMS and 15<\/sup>N relative to liquid ammonia<\/p>\n

2<\/sup> Number of individual chemical shift data for averaging according to [2]<\/p>\n

3<\/sup> with Alanine as neighborhood in the hexapeptide Gly-Gly-X-Ala-Gly-Gly [3]<\/p>\n

4<\/sup> with Proline as neighborhood in the hexapeptide Gly-Gly-X-Pro-Gly-Gly [3]<\/p>\n

5<\/sup> standard deviation<\/p>\n

\n

3D- Modell<\/h3>\n
<\/div>\n

<\/p>\n

sources:<\/p>\n

[1] “BioMagResBank”, Eldon L. Ulrich; Hideo Akutsu; Jurgen F. Doreleijers; Yoko Harano; Yannis E. Ioannidis; Jundong Lin; Miron Livny; Steve Mading; Dimitri Maziuk; Zachary Miller; Eiichi Nakatani; Christopher F. Schulte; David E. Tolmie; R. Kent Wenger; Hongyang Yao; John L. Markley; Nucleic Acids Research 36, D402-D408 (2008) doi: 10.1093\/nar\/gkm957<\/p>\n

[2] http:\/\/www.bmrb.wisc.edu\/ last visit march 2017<\/p>\n

[3] David S. Wishart, Colin G. Bigam, Arne Holm, Robert S. Hodges, Brian D. Sykes; Journal of Biomolecular NMR
\nJanuary 1995, Volume 5, Issue 1, pp 67-81 doi:10.1007\/BF00227471<\/p>\n

[4] Wikipedia\u00a0http:\/\/de.wikipedia.org\/wiki\/Aminos%C3%A4uren (last visit january 2014)<\/p>\n

[5] Wikipedia http:\/\/de.wikipedia.org\/wiki\/Asparagin\u00a0(last visit january 2014)<\/p>\n

3D Mol: Nicholas Rego and David Koes
\n3Dmol.js: molecular visualization with WebGL
\nBioinformatics (2015) 31 (8): 1322-1324 doi:10.1093\/bioinformatics\/btu829<\/p>\n","protected":false},"excerpt":{"rendered":"

NMR- data [1] of lysine: Atom Atomtyp Chemical shift [ppm]1 Random Coil chem. shift3 Random Coil chem. shift4 average \u03c35 entries2 H H \u00a08.178 \u00a00.664 \u00a058906 \u00a08.29 \u00a08.18 H\u03b1 H \u00a04.264 \u00a00.466 \u00a045467 \u00a04.32 \u00a04.60 H\u03b22 H \u00a01.774 \u00a00.319 \u00a041062 \u00a01.84 \u00a01.80 H\u03b23 H \u00a01.744 \u00a00.334 \u00a038519 \u00a01.75 \u00a01.74 H\u03b32 H \u00a01.364 \u00a00.312 \u00a037233 \u00a01.44 … <\/p>\n

Continue reading<\/a><\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"wprm-recipe-roundup-name":"","wprm-recipe-roundup-description":"","jetpack_post_was_ever_published":false,"_jetpack_newsletter_access":"","_jetpack_dont_email_post_to_subs":false,"_jetpack_newsletter_tier_id":0,"_jetpack_memberships_contains_paywalled_content":false,"_jetpack_memberships_contains_paid_content":false,"footnotes":"","jetpack_publicize_message":"","jetpack_publicize_feature_enabled":true,"jetpack_social_post_already_shared":true,"jetpack_social_options":{"image_generator_settings":{"template":"highway","default_image_id":0,"font":"","enabled":false},"version":2}},"categories":[5,4],"tags":[98,110,99],"class_list":["post-1554","post","type-post","status-publish","format-standard","hentry","category-nmr","category-spectroscopy","tag-bio-nmr","tag-lysine","tag-nmr","item-wrap"],"yoast_head":"\nLysine (Lys, K) - 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