{"id":1528,"date":"2017-03-06T16:32:07","date_gmt":"2017-03-06T14:32:07","guid":{"rendered":"https:\/\/wissen.science-and-fun.de\/chemistry\/?p=1528"},"modified":"2017-04-29T10:46:14","modified_gmt":"2017-04-29T08:46:14","slug":"asparagine-asn-n","status":"publish","type":"post","link":"https:\/\/wissen.science-and-fun.de\/chemistry\/2017\/03\/06\/asparagine-asn-n\/","title":{"rendered":"Asparagine (Asn, N)"},"content":{"rendered":"<h3>Overview NMR-Data [1] Asparagine:<\/h3>\n<table border=\"1\">\n<tbody>\n<tr>\n<th rowspan=\"14\"><img data-recalc-dims=\"1\" loading=\"lazy\" decoding=\"async\" class=\"alignleft size-full wp-image-5980\" src=\"https:\/\/i0.wp.com\/wissen.science-and-fun.de\/wp-content\/uploads\/2014\/01\/asparagin.png?resize=149%2C101&#038;ssl=1\" alt=\"asparagin\" width=\"149\" height=\"101\" \/><\/th>\n<th rowspan=\"2\" valign=\"top\">Atom<\/th>\n<th rowspan=\"2\" valign=\"top\">Atomtyp<\/th>\n<th colspan=\"3\">Chemical shift[ppm]<sup>1<\/sup><\/th>\n<th rowspan=\"2\">Random Coil<br \/>\nchem. shift\u00a0<sup>3<\/sup><\/th>\n<th rowspan=\"2\">Random Coil<br \/>\nchem. shift\u00a0<sup>4<\/sup><\/th>\n<\/tr>\n<tr>\n<td><strong>average<\/strong><\/td>\n<td><strong>standard deviation<\/strong><\/td>\n<td><strong>entries<sup>2<\/sup><\/strong><\/td>\n<\/tr>\n<tr>\n<td>H<\/td>\n<td>H<\/td>\n<td>8.349<\/td>\n<td>\u00a02.572<\/td>\n<td>\u00a033343<\/td>\n<td>\u00a08.40<\/td>\n<td>\u00a08.37<\/td>\n<\/tr>\n<tr>\n<td>H\u03b1<\/td>\n<td>H<\/td>\n<td>4.663<\/td>\n<td>\u00a00.367<\/td>\n<td>\u00a026049<\/td>\n<td>\u00a04.74<\/td>\n<td>\u00a05.00<\/td>\n<\/tr>\n<tr>\n<td>H\u03b22<\/td>\n<td>H<\/td>\n<td>2.801<\/td>\n<td>\u00a00.335<\/td>\n<td>\u00a024527<\/td>\n<td>\u00a02.83<\/td>\n<td>\u00a02.82<\/td>\n<\/tr>\n<tr>\n<td>H\u03b23<\/td>\n<td>H<\/td>\n<td>2.744<\/td>\n<td>\u00a00.365<\/td>\n<td>\u00a023670<\/td>\n<td>\u00a02.75<\/td>\n<td>\u00a02.67<\/td>\n<\/tr>\n<tr>\n<td>H\u03b421<\/td>\n<td>H<\/td>\n<td>7.341<\/td>\n<td>\u00a00.916<\/td>\n<td>\u00a018777<\/td>\n<td>\u00a07.59<\/td>\n<td>\u00a07.60<\/td>\n<\/tr>\n<tr>\n<td>H\u03b422<\/td>\n<td>H<\/td>\n<td>7.148<\/td>\n<td>\u00a00.933<\/td>\n<td>\u00a018559<\/td>\n<td>\u00a06.91<\/td>\n<td>\u00a06.92<\/td>\n<\/tr>\n<tr>\n<td>C<\/td>\n<td>C<\/td>\n<td>175.235<\/td>\n<td>3.259<\/td>\n<td>\u00a020665<\/td>\n<td>\u00a0175.2<\/td>\n<td>\u00a0173.6<\/td>\n<\/tr>\n<tr>\n<td>C\u03b1<\/td>\n<td>C<\/td>\n<td>53.538<\/td>\n<td>1.989<\/td>\n<td>\u00a028933<\/td>\n<td>\u00a053.1<\/td>\n<td>\u00a051.3<\/td>\n<\/tr>\n<tr>\n<td>C\u03b2<\/td>\n<td>C<\/td>\n<td>38.702<\/td>\n<td>\u00a02.026<\/td>\n<td>\u00a027479<\/td>\n<td>\u00a038.9<\/td>\n<td>\u00a038.7<\/td>\n<\/tr>\n<tr>\n<td>C\u03b3<\/td>\n<td>C<\/td>\n<td>176.396<\/td>\n<td>\u00a07.175<\/td>\n<td>2125<\/td>\n<td>\u00a0177.2<\/td>\n<td>\u00a0177.1<\/td>\n<\/tr>\n<tr>\n<td>N<\/td>\n<td>N<\/td>\n<td>118.896<\/td>\n<td>\u00a04.414<\/td>\n<td>\u00a027893<\/td>\n<td>\u00a0118.7<\/td>\n<td>\u00a0119.0<\/td>\n<\/tr>\n<tr>\n<td>N<\/td>\n<td>N<\/td>\n<td>112.891<\/td>\n<td>11.509<\/td>\n<td>\u00a016081<\/td>\n<td>\u00a0112.7<\/td>\n<td>\u00a0112.8<\/td>\n<\/tr>\n<tr>\n<th>proportion of proteines<\/th>\n<th colspan=\"2\">pK<sub>2<\/sub> COOH<\/th>\n<th>pK<sub>1<\/sub>COOH<\/th>\n<th colspan=\"2\">\n<table border=\"1\">\n<tbody>\n<tr>\n<th colspan=\"2\">isoelectrical point<\/th>\n<\/tr>\n<\/tbody>\n<\/table>\n<\/th>\n<th>pK<sub>1<\/sub>NH<sub>2<\/sub><\/th>\n<th>pK<sub>2<\/sub>NH<sub>2<\/sub><\/th>\n<\/tr>\n<tr>\n<td>\u00a04,4%<\/td>\n<td colspan=\"2\">\u00a0&#8211;<\/td>\n<td>\u00a02.02<\/td>\n<td colspan=\"2\">\u00a05.41<\/td>\n<td>\u00a08.80<\/td>\n<td>\u00a0&#8211;<\/td>\n<\/tr>\n<tr>\n<th>CAS- number<\/th>\n<th colspan=\"2\">molar mass<\/th>\n<th>formula<\/th>\n<th colspan=\"2\">density<\/th>\n<th>melting point<\/th>\n<th>solubility<\/th>\n<\/tr>\n<tr>\n<td>\n<ul>\n<li>70-47-3 (<small>L<\/small>-Enantiomer)<\/li>\n<li>2058-58-4 (<small>D<\/small>-Enantiomer)<\/li>\n<li>3130-87-8 (<small>DL<\/small>&#8211; Asparagine)<\/li>\n<\/ul>\n<\/td>\n<td colspan=\"2\">\u00a0132,12\u00a0<a title=\"Gramm\" href=\"http:\/\/de.wikipedia.org\/wiki\/Gramm\">g<\/a>\u00b7mol<sup>\u22121<\/sup><\/td>\n<td>\u00a0C<sub>4<\/sub>H<sub>8<\/sub>N<sub>2<\/sub>O<sub>3<\/sub><\/td>\n<td colspan=\"2\"><\/td>\n<td>\n<ul>\n<li>234\u2013236\u00a0\u00b0C\u00a0(<small>L<\/small>&#8211; Asparagine)<sup id=\"cite_ref-Alfa_1-1\"><a href=\"http:\/\/de.wikipedia.org\/wiki\/Asparagin#cite_note-Alfa-1\"><br \/>\n<\/a><\/sup><\/li>\n<li>182\u00a0\u00b0C (Racemat)<\/li>\n<\/ul>\n<\/td>\n<td>\u00a0not good in Wasser (22\u00a0g\u00b7l<sup>\u22121<\/sup>\u00a0for 20\u00a0\u00b0C, Monohydrat)<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<hr \/>\n<p><sup>1<\/sup> Depending on the type of atom it was <sup>1<\/sup>H, <sup>13<\/sup>C or <sup>15<\/sup>N chemical shift. <sup>1<\/sup>H und <sup>13<\/sup>C relative to TMS and <sup>15<\/sup>N relative to liquid ammonia<\/p>\n<p><sup>2<\/sup> Number of individual chemical shift data for averaging according to [2]<\/p>\n<p><sup>3<\/sup> with Alanine as neighborhood in the hexapeptide Gly-Gly-X-Ala-Gly-Gly [3]<\/p>\n<p><sup>4<\/sup> with Proline as neighborhood in the hexapeptide Gly-Gly-X-Pro-Gly-Gly [3]<\/p>\n<hr>\n<h3>3D- Modell<\/h3>\n<div style=\"height: 400px; width: 400px; border-style: solid; position: relative;\" class='viewer_3Dmoljs' data-href='https:\/\/wissen.science-and-fun.de\/molekel\/asparagin.sdf' data-backgroundcolor='0xffffff' data-style='stick' data-typ='sdf'><\/div>\n<p><\/p>\n<p>sources:<\/p>\n<p>[1] &#8220;BioMagResBank&#8221;, Eldon L. Ulrich; Hideo Akutsu; Jurgen F. Doreleijers; Yoko Harano; Yannis E. Ioannidis; Jundong Lin; Miron Livny; Steve Mading; Dimitri Maziuk; Zachary Miller; Eiichi Nakatani; Christopher F. Schulte; David E. Tolmie; R. Kent Wenger; Hongyang Yao; John L. Markley; Nucleic Acids Research 36, D402-D408 (2008) doi: 10.1093\/nar\/gkm957<\/p>\n<p>[2] http:\/\/www.bmrb.wisc.edu\/ last visit march 2017<\/p>\n<p>[3] David S. Wishart, Colin G. Bigam, Arne Holm, Robert S. Hodges, Brian D. Sykes; Journal of Biomolecular NMR<br \/>\nJanuary 1995, Volume 5, Issue 1, pp 67-81 doi:10.1007\/BF00227471<\/p>\n<p>[4] Wikipedia\u00a0http:\/\/de.wikipedia.org\/wiki\/Aminos%C3%A4uren (last visit january 2014)<\/p>\n<p>[5] Wikipedia http:\/\/de.wikipedia.org\/wiki\/Asparagin\u00a0(last visit january 2014) <\/p>\n<p>3D Mol: Nicholas Rego and David Koes<br \/>\n3Dmol.js: molecular visualization with WebGL<br \/>\nBioinformatics (2015) 31 (8): 1322-1324 doi:10.1093\/bioinformatics\/btu829<\/p>\n","protected":false},"excerpt":{"rendered":"<p>Overview NMR-Data [1] Asparagine: Atom Atomtyp Chemical shift[ppm]1 Random Coil chem. shift\u00a03 Random Coil chem. shift\u00a04 average standard deviation entries2 H H 8.349 \u00a02.572 \u00a033343 \u00a08.40 \u00a08.37 H\u03b1 H 4.663 \u00a00.367 \u00a026049 \u00a04.74 \u00a05.00 H\u03b22 H 2.801 \u00a00.335 \u00a024527 \u00a02.83 \u00a02.82 H\u03b23 H 2.744 \u00a00.365 \u00a023670 \u00a02.75 \u00a02.67 H\u03b421 H 7.341 \u00a00.916 \u00a018777 \u00a07.59 \u00a07.60 &hellip; <\/p>\n<p><a class=\"more-link btn\" href=\"https:\/\/wissen.science-and-fun.de\/chemistry\/2017\/03\/06\/asparagine-asn-n\/\">Continue reading<\/a><\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"wprm-recipe-roundup-name":"","wprm-recipe-roundup-description":"","_jetpack_newsletter_access":"","_jetpack_dont_email_post_to_subs":false,"_jetpack_newsletter_tier_id":0,"_jetpack_memberships_contains_paywalled_content":false,"_jetpack_memberships_contains_paid_content":false,"footnotes":"","jetpack_publicize_message":"","jetpack_publicize_feature_enabled":true,"jetpack_social_post_already_shared":true,"jetpack_social_options":{"image_generator_settings":{"template":"highway","default_image_id":0,"font":"","enabled":false},"version":2},"jetpack_post_was_ever_published":false},"categories":[5,4],"tags":[100,98,99],"class_list":["post-1528","post","type-post","status-publish","format-standard","hentry","category-nmr","category-spectroscopy","tag-asparagine","tag-bio-nmr","tag-nmr","item-wrap"],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v27.6 - 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