{"id":1519,"date":"2017-03-06T15:45:00","date_gmt":"2017-03-06T13:45:00","guid":{"rendered":"https:\/\/wissen.science-and-fun.de\/chemistry\/?p=1519"},"modified":"2017-03-06T16:33:10","modified_gmt":"2017-03-06T14:33:10","slug":"1519","status":"publish","type":"post","link":"https:\/\/wissen.science-and-fun.de\/chemistry\/2017\/03\/06\/1519\/","title":{"rendered":"Arginine (Arg, R)"},"content":{"rendered":"

Overview\u00a0NMR-Data [1] for\u00a0Arginine:<\/h3>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
\"arginin\"<\/th>\nAtom<\/th>\nAtomtyp<\/th>\nChemical Shift [ppm]1<\/sup><\/th>\nRandom Coil
\nchem. shift\u00a03<\/sup><\/th>\n		Random Coil
\nchem. shift4<\/sup><\/th>\n<\/tr>\n
average<\/strong><\/td>\nstandard deviation<\/strong><\/td>\nentries2<\/sup><\/strong><\/td>\n<\/tr>\n
H<\/td>\nH<\/td>\n8.24<\/td>\n0.627<\/td>\n40130<\/td>\n\u00a08.23<\/td>\n\u00a08.20<\/td>\n<\/tr>\n
H\u03b1<\/td>\nH<\/td>\n4.293<\/td>\n0.476<\/td>\n31190<\/td>\n\u00a04.34<\/td>\n\u00a04.65<\/td>\n<\/tr>\n
H\u03b22<\/td>\nH<\/td>\n1.789<\/td>\n0.323<\/td>\n28470<\/td>\n\u00a01.86<\/td>\n\u00a01.81<\/td>\n<\/tr>\n
H\u03b23<\/td>\nH<\/td>\n1.756<\/td>\n0.336<\/td>\n26878<\/td>\n\u00a01.76<\/td>\n\u00a01.81<\/td>\n<\/tr>\n
H\u03b32<\/td>\nH<\/td>\n1.558<\/td>\n0.287<\/td>\n25624<\/td>\n\u00a01.63<\/td>\n\u00a01.67<\/td>\n<\/tr>\n
H\u03b33<\/td>\nH<\/td>\n1.537<\/td>\n0.302<\/td>\n23633<\/td>\n\u00a01.63<\/td>\n\u00a01.67<\/td>\n<\/tr>\n
H\u03b42<\/td>\nH<\/td>\n3.106<\/td>\n0.274<\/td>\n25181<\/td>\n\u00a03.20<\/td>\n\u00a03.21<\/td>\n<\/tr>\n
H\u03b43<\/td>\nH<\/td>\n3.089<\/td>\n0.295<\/td>\n22830<\/td>\n\u00a03.20<\/td>\n\u00a03.21<\/td>\n<\/tr>\n
H\u03b5<\/td>\nH<\/td>\n7.469<\/td>\n3.158<\/td>\n8731<\/td>\n\u00a08.07<\/td>\n\u00a08.07<\/td>\n<\/tr>\n
H\u03b711<\/td>\nH<\/td>\n6.915<\/td>\n0.56<\/td>\n821<\/td>\n<\/td>\n<\/td>\n<\/tr>\n
H\u03b712<\/td>\nH<\/td>\n6.846<\/td>\n0.500<\/td>\n625<\/td>\n<\/td>\n<\/td>\n<\/tr>\n
H\u03b721<\/td>\nH<\/td>\n6.801<\/td>\n0.676<\/td>\n701<\/td>\n<\/td>\n<\/td>\n<\/tr>\n
H\u03b722<\/td>\nH<\/td>\n6.877<\/td>\n2.300<\/td>\n579<\/td>\n<\/td>\n<\/td>\n<\/tr>\n
C<\/td>\nC<\/td>\n176.39<\/td>\n3.391<\/td>\n24360<\/td>\n\u00a0176.3<\/td>\n\u00a0174.5<\/td>\n<\/tr>\n
C\u03b1<\/td>\nC<\/td>\n56.77<\/td>\n2.442<\/td>\n34263<\/td>\n\u00a056.0<\/td>\n\u00a054.0<\/td>\n<\/tr>\n
C\u03b2<\/td>\nC<\/td>\n30.72<\/td>\n2.161<\/td>\n32008<\/td>\n\u00a030.9<\/td>\n\u00a030.2<\/td>\n<\/tr>\n
C\u03b3<\/td>\nC<\/td>\n27.23<\/td>\n1.678<\/td>\n20933<\/td>\n\u00a027.1<\/td>\n\u00a026.8<\/td>\n<\/tr>\n
C\u03b4<\/td>\nC<\/td>\n43.169<\/td>\n1.54<\/td>\n21197<\/td>\n\u00a043.3<\/td>\n\u00a043.4<\/td>\n<\/tr>\n
C\u03b6<\/td>\nC<\/td>\n160.246<\/td>\n6.468<\/td>\n566<\/td>\n\u00a0159.5<\/td>\n\u00a0159.6<\/td>\n<\/tr>\n
N<\/td>\nN<\/td>\n120.758<\/td>\n4.197<\/td>\n36557<\/td>\n\u00a0120.5<\/td>\n\u00a0121.3<\/td>\n<\/tr>\n
N\u03b5<\/td>\nN<\/td>\n90.604<\/td>\n13.498<\/td>\n5550<\/td>\n<\/td>\n<\/td>\n<\/tr>\n
N\u03b71<\/td>\nN<\/td>\n79.911<\/td>\n13.90<\/td>\n214<\/td>\n<\/td>\n<\/td>\n<\/tr>\n
N\u03b72<\/td>\nN<\/td>\n79.555<\/td>\n15.263<\/td>\n188<\/td>\n<\/td>\n<\/td>\n<\/tr>\n
proportion of proteines<\/th>\n\u00a0pK2<\/sub> COOH<\/th>\npK1<\/sub>COOH<\/th>\nisoelectrical point<\/th>\npK1<\/sub>NH2<\/sub><\/th>\npK2<\/sub>NH2<\/sub><\/th>\n<\/tr>\n
\u00a04.7%<\/td>\n\u00a0–<\/td>\n\u00a02.81<\/td>\n\u00a011.76<\/td>\n\u00a09.09<\/td>\n\u00a013.2<\/td>\n<\/tr>\n
CAS- number<\/th>\n\u00a0molar mass<\/th>\nformula<\/th>\ndensity<\/th>\nmelting point<\/th>\nsolubility<\/th>\n<\/tr>\n
\n
    \n
  • 74-79-3 (L<\/small>– Arginine)<\/li>\n
  • 1119-34-2 (L<\/small>-Arginine \u00b7Hydrochlorid)<\/li>\n
  • 332360-01-7 (DL<\/small>-Arginine \u00b7Hydrochlorid\u00b7Hydrat)<\/li>\n
  • 157-06-2 (D<\/small>– Arginine)<\/li>\n<\/ul>\n<\/td>\n
\n\n\u00a00,7 g\u00b7cm\u22123<\/sup><\/td>\n\u00a0238\u00a0\u00b0C<\/a><\/td>\n\u00a0good in water (150 g\u00b7l\u22121<\/sup>\u00a0for 20 \u00b0C)<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n
\n

1<\/sup> Depending on the type of atom it was 1<\/sup>H, 13<\/sup>C or 15<\/sup>N chemical shift. 1<\/sup>H und 13<\/sup>C relative to TMS and 15<\/sup>N relative to liquid ammonia<\/p>\n

2<\/sup> Number of individual chemical shift data for averaging according to [2]<\/p>\n

3<\/sup> with Alanine as neighborhood in the hexapeptide Gly-Gly-X-Ala-Gly-Gly [3]<\/p>\n

4<\/sup> with Proline as neighborhood in the hexapeptide Gly-Gly-X-Pro-Gly-Gly [3]<\/p>\n

sources:<\/p>\n

[1] “BioMagResBank”, Eldon L. Ulrich; Hideo Akutsu; Jurgen F. Doreleijers; Yoko Harano; Yannis E. Ioannidis; Jundong Lin; Miron Livny; Steve Mading; Dimitri Maziuk; Zachary Miller; Eiichi Nakatani; Christopher F. Schulte; David E. Tolmie; R. Kent Wenger; Hongyang Yao; John L. Markley; Nucleic Acids Research 36, D402-D408 (2008) doi: 10.1093\/nar\/gkm957<\/p>\n

[2] http:\/\/www.bmrb.wisc.edu\/ last visit march 2017<\/p>\n

[3] David S. Wishart, Colin G. Bigam, Arne Holm, Robert S. Hodges, Brian D. Sykes; Journal of Biomolecular NMR
\nJanuary 1995, Volume 5, Issue 1, pp 67-81 doi:10.1007\/BF00227471<\/p>\n

[4] Wikipedia\u00a0http:\/\/de.wikipedia.org\/wiki\/Aminos%C3%A4uren (last visit january 2014)<\/p>\n

[5] Wikipedia hhttp:\/\/de.wikipedia.org\/wiki\/Arginin (last visit january 2014)<\/p>\n","protected":false},"excerpt":{"rendered":"

Overview\u00a0NMR-Data [1] for\u00a0Arginine: Atom Atomtyp Chemical Shift [ppm]1 Random Coil chem. shift\u00a03 Random Coil chem. shift4 average standard deviation entries2 H H 8.24 0.627 40130 \u00a08.23 \u00a08.20 H\u03b1 H 4.293 0.476 31190 \u00a04.34 \u00a04.65 H\u03b22 H 1.789 0.323 28470 \u00a01.86 \u00a01.81 H\u03b23 H 1.756 0.336 26878 \u00a01.76 \u00a01.81 H\u03b32 H 1.558 0.287 25624 \u00a01.63 \u00a01.67 … <\/p>\n

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