{"id":751,"date":"2013-12-14T07:38:36","date_gmt":"2013-12-14T05:38:36","guid":{"rendered":"https:\/\/wissen.science-and-fun.de\/chemistry\/?page_id=751"},"modified":"2013-12-14T08:11:33","modified_gmt":"2013-12-14T06:11:33","slug":"important-silylated-compounds-used-as-1h-shift-references","status":"publish","type":"page","link":"https:\/\/wissen.science-and-fun.de\/chemistry\/spectroscopy\/important-silylated-compounds-used-as-1h-shift-references\/","title":{"rendered":"Important Silylated Compounds used as 1H Shift References"},"content":{"rendered":"\n\n\n\n\t\n\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t\n\t
Name<\/th>Chemical Formula<\/th>Abbreviation<\/th>Molecular weigth<\/th>Boiling or Melting Point (\u00b0C)<\/th>δ 1<\/sup>H ppm (rel. TMS)<\/th>\n<\/tr>\n<\/thead>\n
Tetramethylsilane<\/td>Me4<\/sub>Si<\/td>TMS<\/td>88.2<\/td>BP=26.3<\/td>0<\/td>\n<\/tr>\n
Hexamethyldisilane<\/td>Me3<\/sub>Si-SiMe3<\/sub><\/td>HMDS<\/td>146.4<\/td>BP=112,3<\/td>0.037<\/td>\n<\/tr>\n
Hexamethyldisiloxane<\/td>Me3<\/sub>Si-O-SiMe3<\/sub><\/td>HMDSO<\/td>162.4<\/td>BP=100<\/td>0.055<\/td>\n<\/tr>\n
Hexamethyldisilazane<\/td>Me3<\/sub>Si-NH-SiMe3<\/sub><\/td>HMDSA<\/td>161.4<\/td>BP=125<\/td>0.042<\/td>\n<\/tr>\n
3-(trimethylsilyl)propane sulfonic acid sodium salt<\/td>Me3<\/sub>Si(CH2<\/sub>)3<\/sub>SO3<\/sub>Na<\/td>TSPSA<\/td>218.3<\/td>MP=200<\/td>0.015<\/td>\n<\/tr>\n
4,4-dimethyl-4-silapentane sodium sulfonate<\/td>DSS<\/td>\n<\/tr>\n
3-(trimethylsilyl)propionic acid sodium salt<\/td>TSP<\/td>\n<\/tr>\n
4,4-dimethyl-4-silapentane sodium carboxylate<\/td>Me3<\/sub>Si(CH2<\/sub>)2<\/sub>COONa<\/td>DSC<\/td>168.2<\/td>MP>300<\/td>0.000<\/td>\n<\/tr>\n
3-(trimethylsilyl)2,2,3,3-tetradeuteropropionic acid sodium salt<\/td>Me3<\/sub>Si(CD2<\/sub>)2<\/sub>COONa<\/td>TSP-d4<\/sub><\/td>172.2<\/td>MP>300<\/td>0.000<\/td>\n<\/tr>\n
Octamethylcyclotetrasiloxane<\/td>\"\"<\/a><\/td>OCTS<\/td>296.8<\/td>BP=175
\nMP=16.8<\/td>		0.085<\/td>\n<\/tr>\n
1,1,3,3,5,5-hexakis-(trideuteromethyl)-1,3,5-trisilacyclohexane<\/td>\"\"<\/a><\/td>CS-d18<\/sub><\/td>216.6<\/td>BP=208<\/td>-0.327<\/td>\n<\/tr>\n
Tetrakis-(trimethylsilyl)-methane<\/td>[Me3<\/sub>Si]4<\/sub>C<\/td>TTSM<\/td>304.8<\/td>MP=307<\/td>0.236<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\nSource: Bruker Almanac 2012<\/span>\n\n","protected":false},"excerpt":{"rendered":"","protected":false},"author":1,"featured_media":0,"parent":7,"menu_order":11,"comment_status":"open","ping_status":"closed","template":"","meta":{"wprm-recipe-roundup-name":"","wprm-recipe-roundup-description":"","jetpack_post_was_ever_published":false,"footnotes":""},"class_list":["post-751","page","type-page","status-publish","hentry","nodate","item-wrap"],"yoast_head":"\nImportant Silylated Compounds used as 1H Shift References - Steffen's Chemistry Pages<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/wissen.science-and-fun.de\/chemistry\/spectroscopy\/important-silylated-compounds-used-as-1h-shift-references\/\" \/>\n<meta property=\"og:locale\" content=\"en_US\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"Important Silylated Compounds used as 1H Shift References - 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